How to efficiently melt down a quartz glass ampoule under vacuum with a oxyhydrogen torch?

Hi chemists of Reddit!

I recently started my bachelor thesis and now have to use a oxyhydrogen torch on a regular basis to seal reactants in a quartz glass ampoule in vacuo. Well it turns out that is kind of tricky. So now I wonder how other people do it?

I was thaught the two-bubble approach, where you would melt two bubbles into the opposite sites of the glass tube until they met in the middle. Then you would melt the edges of the bubbles to that ideally you have one flat wide and one narrow side. Afterwards you take the flask off the Schlenk line (but of course keep the vacuum) and start working on heating the section you "prepared" and slowly pulling it apart.

I already burned one or two holes into my ampoules, which basically means having to start all over, so I am very grateful for any tips and other people's experiences :)


Clarification: I am of course supervised and no one is alone in the lab while working with the torch :) And they are all very nice and have their routines doing it and happily give advice.

I already did about four, the first one empty for practice, all while wearing the appropriate goggles and gloves.

I mostly am interested what techniques other labs use, does everyone have their own? I found one video of a man just burning trough his ampoule in two minutes, while we need 10-20min and wonder whether that really works.. it looked like he should have burned through the glass in seconds, but seemed to have been successful.

The video: https://av.tib.eu/media/18717 (at 10:45min)

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If you need any more information, tell me!

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Thanks in advance...

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